Experiments in LED encapsulation

saabluster

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This is something I have been wanting to do a while and bought the material quite some time ago do a project using quantum dots but those will have to wait. I have been wanting to encapsulate my own LEDs to do experiments on what the absolute best setup is for my aspheric setup. I have not had time yet to run any tests but I got some pictures today and thought I'd get it started. I am using a high grade optical silicone meant for encapsulating LEDs. This is not Home Depo material here. I removed the domes of both LEDs and scraped off the silicone gel down to the silicone layer that holds the phosphor.


From left to right we have an XR-E with an acrylic optic applied over the encapsulant, a regular XR-E, and an XR-E with only silicone encapsulant. Notice how you can already see the LED die on the one with the acrylic optic.
PICT0117.jpg


See the change in die size?
PICT0109-1.jpg


PICT0104-1.jpg


PICT0111-1.jpg


I'll have to get to the tests at a later date.
 
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bshanahan14rulz

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Re: DIY LED encapsulation

why the dome? Why not just a flat layer of silicon encapsulant? That would make your die appear even smaller, right?

(btw, I'm trying to make a P60 drop-in, just waiting to find a suitable chunk of copper that would put the die in the focal point of the smo reflector. It would be nice to encapsulate the die, only for protection, since my whole reason for doing this was decreasing the die size and putting more light to the reflector. I was just wondering if you've done any lumens testing of LED with and without dome. It is common knowledge that an LED will dim and change colors when you remove the dome and the gel. However, I don't believe it at all, since mine didn't change colors and definitely appears brighter (smaller point). right now, I'm not able to afford to buy any parts, hence the wait for a suitable chunk of metal to show up, but I was mainly curious if you've noticed any degradation of light output or tint. Oh, and I guess I'll close my parenthesis...)
 

saabluster

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Re: DIY LED encapsulation

why the dome? Why not just a flat layer of silicon encapsulant? That would make your die appear even smaller, right?

(btw, I'm trying to make a P60 drop-in, just waiting to find a suitable chunk of copper that would put the die in the focal point of the smo reflector. It would be nice to encapsulate the die, only for protection, since my whole reason for doing this was decreasing the die size and putting more light to the reflector. I was just wondering if you've done any lumens testing of LED with and without dome. It is common knowledge that an LED will dim and change colors when you remove the dome and the gel. However, I don't believe it at all, since mine didn't change colors and definitely appears brighter (smaller point). right now, I'm not able to afford to buy any parts, hence the wait for a suitable chunk of metal to show up, but I was mainly curious if you've noticed any degradation of light output or tint. Oh, and I guess I'll close my parenthesis...)

I made it the shape of a dome because the LED is going to be aiming at an optic and I wanted the escape surfaces to be as perpendicular as possible to reduce the chance of internal reflection. Don't know if it is a success or not yet as I have not done any testing. BTW removing the dome of an XR-E does cause a loss of lumens of about 30%. The fact that the beam is smaller does not mean it is bright- just small. You may have pulled yours off very cleanly and that helped keep it from changing tint.

Heres hoping it rains copper near you some time soon.:D
 

bshanahan14rulz

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Re: DIY LED encapsulation

I wanted the escape surfaces to be as perpendicular as possible to reduce the chance of internal reflection
Ahh, makes complete sense! dome ensures light hits the intersection "plane" of gel and air at close to perp for maximum light transmission and minimal internal reflection, so it's all about finding the perfect combo of small source but also high light extraction percentage. Ok, how bout this one: I've heard that the metal ring actually is meant to reflect light forward. Is this like, an afterthought, or a gimmick to increase the final numbers for total emitter lumens? as this light doesn't seem like it's very usable, and usually just makes a different-color ring around the beam. If you encapsulated it w/o the ring, though, you'd have to make the dome more domed, hence larger die image though, right? ok, so you don't have to answer that one after all.

BTW removing the dome of an XR-E does cause a loss of lumens of about 30%.
Ah, dern. Well, 30% of an R2 isn't too bad, I guess. Do you think if I get this LED spaced right, it will throw better than a complete cree LED with the same SMO reflector?

Heres hoping it rains copper near you some time soon.:D
Thanks! I have found some cheapo server heatsinks, stacked fins, soldered onto 5mm thick copper, might try to find a way to get at that copper. Don't have a torch, so desoldering is out of the question. I sure would like to get my hands on some of those solid, 1pc copper skivved sinks that we replaced these with :naughty:

Ever thought about developing a TIR mold and just encapsulating the LED and make the optic at the same time? Although from the sound of it, this encapsulant you're using is top-o-the-line $$$ stuff..
 
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saabluster

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Re: DIY LED encapsulation

Ok, how bout this one: I've heard that the metal ring actually is meant to reflect light forward. Is this like, an afterthought, or a gimmick to increase the final numbers for total emitter lumens? as this light doesn't seem like it's very usable, and usually just makes a different-color ring around the beam.
It's no gimmick. In a fixture that mixes or diffuses the light the ring is a non-issue and the added light is a good thing. They did not have just flashlights in mind when they designed the XR-E.

If you encapsulated it w/o the ring, though, you'd have to make the dome more domed, hence larger die image though, right? ok, so you don't have to answer that one after all.
Well you don't have to make it more domed. I personally want the surface as far from the die as possible for the same reason I am shooting for a flatter surface. I would not need to do this if the die was a true point source.

Ah, dern. Well, 30% of an R2 isn't too bad, I guess. Do you think if I get this LED spaced right, it will throw better than a complete cree LED with the same SMO reflector?
Quite possibly yes. That is if you are comparing the modified XR-E to a normal XR-E. I would not expect it to throw more than an XP-E though. Only one way to know for sure though.:poke:


Ever thought about developing a TIR mold and just encapsulating the LED and make the optic at the same time? Although from the sound of it, this encapsulant you're using is top-o-the-line $$$ stuff..
Yes. Many times. This is more of a task than I have time for right now though.
 

Gomer

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Re: DIY LED encapsulation

how about eliminating the dome all together and use a TIR optic and index match (well, close) between the dome and the lens?
 

saabluster

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Re: DIY LED encapsulation

how about eliminating the dome all together and use a TIR optic and index match (well, close) between the dome and the lens?
Because the TIR optic would have to be designed specifically for that. There is no such thing as far as I know.
 

lolzertank

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Re: DIY LED encapsulation

Would TFFC Rebels be better for doing this? After all, they don't have any fragile bond wires to break like the XR-Es. I guess a ring could be added to focus the light.
 

saabluster

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Re: DIY LED encapsulation

Would TFFC Rebels be better for doing this? After all, they don't have any fragile bond wires to break like the XR-Es. I guess a ring could be added to focus the light.
No they would not be any better than the XR-E as it is really easy to get all the gel off the XR-E die without damaging the phosphor. Seems like it is fairly easy to pull off the phosphor layer on the rebels. I'm just going by memory from others experience. I don't have any experience destroying rebels. In any case the XR-E can handle more power so it is my preferred platform.

What do mean a ring could be added?
 

saabluster

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Re: DIY LED encapsulation

I'm talking about the reflective ring on the XR-E, but since you're going to stick with XR-Es, it doesn't really matter.
Oh were you talking about adding a ring to the Rebels?



Hoping for an XR-G! :eek:
Me toooooo. Want to go camp outside Cree together and protest until they release one? :hitit:
 

saabluster

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I have now taken some tests both empirically and with my lux meter. I installed each one in a DEFT and tested side by side. The LED that had the silicone alone(the one on the star) did horrible enough by eye that I didn't even bother testing with the meter. This does not mean that the encapsulation method is to blame however as it was an old LED of unknown bin or provenance. I think it was a Q5 WC but the output from it was feeble so there may have been some abuse imparted upon it by myself sometime in the past.

Anyway I took the lights outside and had a normal DEFT as the control. The normal DEFT and the acrylic modified LED were both R2 WHs. I am stunned to say it but the one with the acrylic threw significantly farther. Judging by my eye I guessed the modified XR-E had just slightly less than twice the intensity of the normal XR-E! I swapped the batteries from one to the other to make sure that was not a factor. No change.

I ran inside and used my light meter to pin down just what the difference was. I did the measurements from about 15' away. The relative throw measurements for them are as follows.

Unmodified XR-E DEFT- 20
Acrylic/silicone encapsulated XR-E in DEFT- 34

This matches exactly what my eyes saw outside. That means I now have a system for an aspheric that beats the lab designed result! Now I need to combine this with the method of reducing the ceramic backer I created and mount it to a heat-pipe. Should be one heck of an LED.

Now if I can just get those quantum dots from our friend here.:whistle: You know who you are.:poke:
 

saabluster

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Well it just gets better and better folks. I think I have made the best LED you could have. In playing with it more I have found it has some unique qualities that are not found in other LEDs. Some people may be aware of how the tint can change on XR-Es when the dome is removed. We don't know for sure why this is but the tint has also changed on my modified XR-E. The strange and wonderful thing is that it has shifted more to the red side. This is the warmest cool white LED I can ever remember seeing. The CRI seems to have improved as well. I took it outside without the head so that it was full flood and it was a thing to behold. It was the best beam I have ever seen from a bare LED. Better rendering of the reds in the fallen leaves was noticeable. One other thing that changed about the beam is the variance in tint dependent on angle of emitted light. The unmolested XR-E has more blue in the center of the output and gets warmer as the angle increases. Not the modified one. Smooth tint throughout the spacial distribution.

I created this as an experiment to create a better LED for aspherics but it works just as well with a reflector. The beam is much tighter and more intense with an incredible tint. It is what I call vanilla white. The only down side is the Cree rings have been "enhanced" in the new setup. With a reflector an orange peel should handle that just fine and I figure on the one for the aspherics I can use a flat black paint on the ring to make it disappear.

I am thoroughly blown away by these results. I didn't expect it to be even half as good as it turned out to be. Now I need to do some more to make sure this wasn't a fluke.
 

Th232

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:eek:
:bow::bow::bow:

Saab, if you manage to get this process down pat, would it be possible for you to sell some of these modified LEDs? I'm currently building an aspheric, and I'd love to get my hands on a couple of those!
 

saabluster

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:eek:
:bow::bow::bow:

Saab, if you manage to get this process down pat, would it be possible for you to sell some of these modified LEDs? I'm currently building an aspheric, and I'd love to get my hands on a couple of those!
The results are so good I am seriously considering offering some for sale. I need to do some more testing to be sure it is fairly reliable but it did wonderfully at 1500mA for about 35 minutes. More testing is obviously in order though. Next I will try an AR coated glass optic. That may actually allow me to have more output than the stock XR-E as my light meter tests suggested I was only losing about 5-6% in total lumens using the acrylic.

Can you imagine an R3 bin XR-E with a super tiny die size and great tint. I'm salivating just thinking about it.:drool:
 

Gryloc

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Saabluster,

Nice work with encapsulating the XR-E emitters. I have been watching this in excitement to see what happens when a flashaholic has control over the emitter dome shape. BTW, how have these mods affected overall lumen output compared to before the mod? I personally lost domes off of two Rebel 0100 emitters and it seems like the phosphor was perfectly intact and the LED operational. The K2, and the Cree products still use bond wires that would be torn after removing the die. Hopefully, regardless of the emitter used, domes will not have to be removed in your experiments. Clean silicone domes of the XP-E, XP-G, and Rebel might disappear when you goop your silicone gel over top of it (so dome removal may be unnecessary).

So, I was just wondering why the encapsulated XR-E (dome removed) with the acrylic lens did better than the one without. Is it an issue with different indexes of refraction? Is it because the acrylic lens has a smoother surface?

You may have stumbled on something good for aspheric lens users, but I think before you should start selling these in large quantities, you should do more testing. I think that members would love to see comparisons between 3-4 new XR-E emitters from the same batch. Who knows, maybe your modded emitter without the lens degraded some, and if in better shape, could have perform the best. Having new emitters that perform the same from the start will help produce more conclusive tests in a more scientific fashion. (I understand the preliminary experiments with spare XR-Es). BTW, does the Deft use a high quality current regulator so even big changes in LED forward voltage will not affect output? I was just wondering.

Between the two modified XR-E emitters, I guess I do not understand why they are so different. Why not remove the ring and then re-encapsulate the emitter? Why not re-encapsulate a Rebel, XP-E or XP-G? I see that the consistency of the optical grade silicone gel causes your "dome" to sag before it cures, but why not let gravity aid you? I do not know its viscosity or its values for surface tension, but maybe when held upside down, a dome might form a geometric shape in your favor (parabolic, spherical, elliptical, or catenary). If you are going for flatness, then why not temporarily fix it to the center flat spot of an old brushless PC cooling fan and let centripetal forces level off the top of the dome some? If the viscosity is high enough and you make the fan spin slow enough, you may get a very flat surface. As you spin it faster it may begin forming a parabolic dip in the center (like what happens with those experimental spinning mercury mirrors). You have a lot of control over the shape of this dome; that is awesome.

If that acrylic lens is the ultimate solution, then why not take an old Cree XR-E metal ring (or a spacer with the same height) and fix it above a Rebel, XP-E, or even XP-G then fix on the acrylic lens? Maybe a modded XP-G would produce a projected beam (in the Deft) of the same size as an un-modded XR-E from your existing setup (I am being hopeful here).

I am just asking that you try different setups with other emitters. We all bow to you since you have the optical grade silicone gel and experience. I like the XR-E, but have always been doubtful to the metal ring from the optical standpoint (I understand the mechanical purposes). If you can make a new dome over the tiny Rebel, XP-E, and XP-G, you might be able to shape the dome to do the same thing that the glass dome on the XR-E did, or you may be able to shrink down the apparent die size (flatten the dome) without sacrificing the total lumen output.

I always found the tint shift interesting. I also worry that the tint shift, while being pleasant to the eyes, may be bad for efficiency or overall longevity. It seems like a major change happens when the tint shift occurs, and it could be a bad change. Does it mean that more blue light is internally reflected back to the phosphor coating to produce reds
(due to the change in index of refraction), or does it maybe affect how heat is removed from the top of the light which affects the efficiency of the phosphors?

Again, good job. Thanks for your patience with my numerous questions mixed in my post. Your experiment is intriguing, as many are afraid of working at the emitter level when doing modifications and experiments. If I had the tools and resources, I would have acted on my own emitter mods. For example. You could theoretically can cut rebel emitters down (the ceramic substrate) without affecting the etched traces to position the four dies tightly together so they almost touch (electrically, they could touch if you plan on wiring the dies in parallel). Just re-encapsulate them (or not if you cut cleanly) and this could equate into a quad TFFC die emitter. Its not a practical mod (with the MC-E, P7, and SST-50 out there), but I dream that it could be done.

Cheers,
-Tony
 

saabluster

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Saabluster,

Nice work with encapsulating the XR-E emitters. I have been watching this in excitement to see what happens when a flashaholic has control over the emitter dome shape. BTW, how have these mods affected overall lumen output compared to before the mod? I personally lost domes off of two Rebel 0100 emitters and it seems like the phosphor was perfectly intact and the LED operational. The K2, and the Cree products still use bond wires that would be torn after removing the die. Hopefully, regardless of the emitter used, domes will not have to be removed in your experiments. Clean silicone domes of the XP-E, XP-G, and Rebel might disappear when you goop your silicone gel over top of it (so dome removal may be unnecessary).
As I mentioned in my last post lumens are down about 5-6% but it's hard to be sure since the spacial distribution is much different and I do not have an IS.
I think you may have misunderstood what I did here. I did remove the dome and removed the gel that sits under the dome in its entirety. I took it all the way down to the phosphor impregnated silicone elastomer(note not the same thing as the gel) that Cree uses to coat the die with. Then I applied my silicone on top. Domes do have to be removed or it will not work. Also I have never had a Cree fail from pulling the dome off. The bond wires are fairly tough. I even picked at one to see how strong it was.

So, I was just wondering why the encapsulated XR-E (dome removed) with the acrylic lens did better than the one without. Is it an issue with different indexes of refraction? Is it because the acrylic lens has a smoother surface?
As I said I don't know what the condition of that LED(silicone only) was prior to the test. It was just sitting in the drawer missing a dome so I used it. This was just a preliminary test to see what would happen to the shape of the beam and get an idea if my ideas for encapsulation would work. There could be issues with index matching to the atmosphere and there may not be. I will not know until I can try it again with a know good LED. The one with the acrylic was known to be good.

You may have stumbled on something good for aspheric lens users, but I think before you should start selling these in large quantities, you should do more testing. I think that members would love to see comparisons between 3-4 new XR-E emitters from the same batch. Who knows, maybe your modded emitter without the lens degraded some, and if in better shape, could have perform the best. Having new emitters that perform the same from the start will help produce more conclusive tests in a more scientific fashion. (I understand the preliminary experiments with spare XR-Es). BTW, does the Deft use a high quality current regulator so even big changes in LED forward voltage will not affect output? I was just wondering.
As I said before more testing is definitely in order. This is also not just good for aspherics as the beam was significantly better for a reflector I used with it. The DEFT's output can change based on Vf and I know that so I will find a more accurate means of testing on the next round. This was just a proof of concept.

Between the two modified XR-E emitters, I guess I do not understand why they are so different. Why not remove the ring and then re-encapsulate the emitter? Why not re-encapsulate a Rebel, XP-E or XP-G? I see that the consistency of the optical grade silicone gel causes your "dome" to sag before it cures, but why not let gravity aid you? I do not know its viscosity or its values for surface tension, but maybe when held upside down, a dome might form a geometric shape in your favor (parabolic, spherical, elliptical, or catenary). If you are going for flatness, then why not temporarily fix it to the center flat spot of an old brushless PC cooling fan and let centripetal forces level off the top of the dome some? If the viscosity is high enough and you make the fan spin slow enough, you may get a very flat surface. As you spin it faster it may begin forming a parabolic dip in the center (like what happens with those experimental spinning mercury mirrors). You have a lot of control over the shape of this dome; that is awesome.
I want the ring there because it performs a function. It holds the lens away from the die and makes sure that it is straight and level. Ideally I'd like it even higher than it is now. That will be in some future tests.
I can create any shape that I want with this stuff. What I had was what I wanted to have. There is no need to spin it to get a flat surface as you can just use less of the encapsulant and surface tension will draw it tight if you have the right amount. That is not what I am after however.

If that acrylic lens is the ultimate solution, then why not take an old Cree XR-E metal ring (or a spacer with the same height) and fix it above a Rebel, XP-E, or even XP-G then fix on the acrylic lens? Maybe a modded XP-G would produce a projected beam (in the Deft) of the same size as an un-modded XR-E from your existing setup (I am being hopeful here).
The reason I am not even considering any of those LEDs is because they have neither the surface brightness nor the ability to over-drive that the XR-E does. Keep in mind I am always searching for a way to improve throw and this is the fundamental starting point for that.

I am just asking that you try different setups with other emitters. We all bow to you since you have the optical grade silicone gel and experience. I like the XR-E, but have always been doubtful to the metal ring from the optical standpoint (I understand the mechanical purposes). If you can make a new dome over the tiny Rebel, XP-E, and XP-G, you might be able to shape the dome to do the same thing that the glass dome on the XR-E did, or you may be able to shrink down the apparent die size (flatten the dome) without sacrificing the total lumen output.
I may try a different emitter some time in the future but for now I am going to stick with the XR-E.

I always found the tint shift interesting. I also worry that the tint shift, while being pleasant to the eyes, may be bad for efficiency or overall longevity. It seems like a major change happens when the tint shift occurs, and it could be a bad change. Does it mean that more blue light is internally reflected back to the phosphor coating to produce reds
(due to the change in index of refraction), or does it maybe affect how heat is removed from the top of the light which affects the efficiency of the phosphors?
I highly doubt there are any ill side effects from the tint shift. I am not losing much in total output at all so there cannot be any real effect of heating up the die or phosphor. Any extra heat at the die level created by my encapsulation method would at worst be like dropping a bin in LED efficiency. I don't see Q5s failing because they are less efficient and create more heat than R2s so I'm not worried.;) It is strange that it shifted more red as whenever I have removed domes from XR-Es in the past(and not re-encapsulated) they turn a **** yellow/green. This is a nice change. It remains to be seen if this happens consistently though. I am sufficiently amazed though as it nows appears as if it is a proper neutral white color. Maybe in 3A territory.
You could theoretically can cut rebel emitters down (the ceramic substrate) without affecting the etched traces to position the four dies tightly together so they almost touch (electrically, they could touch if you plan on wiring the dies in parallel). Just re-encapsulate them (or not if you cut cleanly) and this could equate into a quad TFFC die emitter. Its not a practical mod (with the MC-E, P7, and SST-50 out there), but I dream that it could be done.

Cheers,
-Tony
That reminds me of another idea I had and still want to try out. The rebels would be ideal for it as well. My idea is to take 5 dies and position them so as to form a box. One would be flat as a normal LED. The other 4 are raised up to form the sides of the box with the top open for light to escape. The idea is that the four LEDs will help add some surface brightness to the base one which is the one the lens would be primarily focused on. You should be able to use an efficient cool white LED and have the resulting tint output to be warmer than it would otherwise. The increase in brightness would be minimal I'm sure but I am looking for any way to get ahead.:D It is just an idea I have had in my head and I have not had a chance to test it out as yet.
 

dom

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Excellent work Saabluster.

Do you think the phosphor being exposed to the air has changed the tint?
In your 2nd picture the color of the top left is slightly darker.

It's a wonder your DEFT customers aren't all over this thread looking for an upgrade! :)

Cheers
Dom
 
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saabluster

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Excellent work Saabluster.

Do you think the phosphor being exposed to the air has changed the tint?
In your 2nd picture the color of the top left is slightly darker.

It's a wonder your DEFT customers aren't all over this thread looking for an upgrade! :)

Cheers
Dom
Even if you remove the silicone gel from off the top of the phosphor the phosphor itself is not coming in contact with air. The phosphor is suspended in a silicone elastomer that acts as a binder.

You may notice that relatively few people come down here to the LED section. It is a place for LED geeks of which group I claim to be a part. Few people here truly understand the magnitude of what's been accomplished here but I'm fine with that. Thanks for noticing.
 
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